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Picric Acid

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(123 votes)
Published: Oct 30, 2006 7:04 p.m.
In 20 Favorites Lists
Viewed 1080 times


picric acid is a really cool substance and quite easy to make it is really powerful and it has many uses. it is made from easily found substances that can be easily obtained from around town



MATERIALS:
potassium nitrate (easily found at any lowes under the name spectracide stump remover http://img247.imageshack.us/my.php?image=stumpremoveryc4.jpg

aspirin (found easily at pretty much any store http://img247.imageshack.us/my.php?image=aspirinchcb2.jpg

mason jar (art and craft stores)

drain cleaner (dollar store supermarket hardware store http://img151.imageshack.us/my.php?image=drainmj0.jpg

oven hotplate, any heat sorce will do preferable make this outside

PROCEDURE: (these are not my pics these are from a friend so im giving him credit for the de5cription and pics)

I used red coloured drain cleaner, recrystallized acetylsalicyclic acid and potassium nitrate in prill form.

First, I put 220ml of drain cleaner in a 700ml jar, and began heating the water bath. As it was heating up, I added 40 grams of ASA (acetylsalicyclic acid or aspirin) and stirred it. It all dissolved once the water bath reached boiling temperature, and during this time the solution turned from red to deep black. After the ASA finished dissolving, I continued heating in the boiling water bath for 25 minutes, with ocassional stirring


http://img246.imageshack.us/my.php?image=sulfonation1flhz6.jpg

I took it out of the boiling water, then proceeded to add potassium nitrate very slowly, at a rate just slow enough to prevent orange fumes from forming. The mixture foamed during this step.



The rate of foaming varied, being strongest near the middle of the addition process then slowing down again near the end. The colour lightened until it had formed a clear red solution. The addition took a total of 40 minutes to complete.
http://img246.imageshack.us/my.php?image=finish3uxll2.jpg

This was allowed to sit for about 15 minutes, after which a layer of yellow picric acid had formed on top. I then stuck it in boiling water for another 6 minutes, and a bit more picric acid was formed.
http://img246.imageshack.us/my.php?image=finish27bnjg1.jpg

I let it cool a bit, then helped it along with some cold water since it was getting late. I then poured the room temperature or therabouts solution in 1 liter of cold water, and then more water was used to rinse out the remaining picric acid out of the nitration jar.
http://img246.imageshack.us/my.php?image=diluted0nrnj0.jpg

filter the yellow cystals on the top of the jar and allow them to dry then light them
please store this in like u tupperware container just incase of a accidental ignition all that would happen woulld the top would fly off

WARNING:

never ever ever store this in a glass jar with a screw on lid if you do the picric acid will recrystalize in the threads of the jar and when open it there will be a accidental ignition caused by the friction on the lid twisting on the jar

thank you and have fun and please be safe
 

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rdawgog

Oct 30, 2006 7:30 pm -
nice egg 5* that shit is extremely explosive, it explodes at a rate of 7,100 m/s and tnt explode at a rate of 6,800 m/s


BiggieSmalls

Oct 30, 2006 7:34 pm -
nice


BadCat

Oct 30, 2006 8:26 pm -
One of the easier ways to make it- 5*s


Over-Dose

Oct 30, 2006 8:28 pm -
What are some use’s for this stuff, oh and good egg,5*.
You should add actuall picture’s and not link’s.


NoMoreWednes ay

Oct 30, 2006 10:39 pm -
^ is this kid a retarded hick?
4****


DarkestAngel

Oc 30, 2006 10:50 pm -
^^^ Watch it buddy, I’m a hick :)


pyrodude-3753

Oct 31, 2006 12:51 pm -
some of the uses for this stuff is like igniters for other less sensitive explosives um lemme think u could use it as a blasting cap just wrap it in a little bit of tin foil and use it like a blasting cap u could use it as a main charge just be very careful and thats about it im sure if u used your imagination u could come up with some good ideas


OnikuraX

Oct 31, 2006 1:02 pm -
wow pretty good =] 5*

*waits for halflifelover’s response*


pyrodude-3753

Oct 31, 2006 4:09 pm -
its a explosive.....i said that before

Oct 31, 2006 4:56 pm -
I really don’t feel like ranting on this one. Can you explain the chemistry behind this? If you can’t, then you shouldn’t be doing this. You do know that the noobs here are going to be blowing the fuck out of everything.


pyrodude-3753

O t 31, 2006 5:37 pm -
well basicly i made this egg because i think its cool and it is very simple just follw the instructions and nothing should go wrong besides i neevr told anyone to make it i neevr put a gun to their head and said make this or die but i understand what u mean and respect your opinion


Salamanderhead

Nov 01, 2006 3:22 am -
lmao, I thought that hotplate was an atari when I first glanced.


nephrosis

Nov 01, 2006 3:48 am -
Quote:
mayb im just stupid but are you trying to make acid to trip on or are you trying to make some bullshit that explodes?

LMAO. Wow...this is why kids die from making explosives. Anyways great egg, I gave you a 5.


Jigsaw

Nov 03, 2006 4:50 pm -
nice egg 5*


JackaI

Nov 06, 2006 6:54 pm -
Nice egg, but this stuff is really dangerous. It has a NPFA flammability rating of 4, which means any can kind of friction can make this stuff react and explode. Be careful, you crazy bastard.


duhtaduh

Nov 25, 2006 1:56 am - Ur smart
Go make a binary explosive u terrorist


HardR0ckPyr0

Jul 16, 2007 11:57 pm -
this is cool shit go to unitednuclear.com and you can LEGALLY buy MERCURY 2oz for $25 no shit and pure acids 35% hydrogen peroxide and THERMITE


Shave_Americas_Bu h-6127

Sep 01, 2007 2:38 pm -
came by to rate this 5 cuz of your sword egg..... Im pretty sure picric acid is used in the production of nitroglycerin.


Warchemy

Sep 02, 2007 7:29 pm -
no, you’re thinking of nitric acid.

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